catalyst: Pd/Ce-Zr-La-γ-alumina in neat (no solvent) Kinetics; byproducts: N2O, NH3, NH2(2)H; Ar; at 155+/-3°C, at atm. pressure; further by-products: NH(2)H2,N(2)H3; MS;
参考文献
Rahkamaa-Tolonen; Salmi; Murzin; Barreto Dillon; Lassi; Keiski
Journal of Catalysis, 2002 , vol. 210, # 2 p. 30 - 38
Noll, J. E.; Speier, J. E.; Daubert, B. F.
Journal of the American Chemical Society, 1951 , vol. 73, p. 3867 - 3871
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Gmelin Handbook: Si: MVol.C, 4, page 14 - 18
in not given H2-atmosphere; stirring Rh-complex with 4 equiv. PPh3 and 0.5 equiv. of PPh2(NC4H4) (in C6D6 or PhMe, not specified); not isolated, detd. by (1)H-, (31)P-NMR spectroscopy;
参考文献
Journal of Organometallic Chemistry, , vol. 552, # 1-2 p. 159 - 164
aluminium; aluminium trichloride in neat (no solvent) byproducts: Al(OC6H5)3; High Pressure; heating to 180°C under 2000 psi H2-pressure for 1h; filtration;; separation of product at 97°C and 2 Torr;;
参考文献
Ashby, E. C.; Foster, W. E.
Journal of the American Chemical Society, 1962 , vol. 84, p. 3407 - 3408
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Gmelin Handbook: B: B-Verb.14, 3.8.1.2.1, page 94 - 97
magnesium; mercury dichloride in 2-methyl cyclohexane byproducts: Mg(O-i-C4H9)2; High Pressure; heating to 300°C under 1825 psi H2 pressure;; separation of product by distn.;;
参考文献
Gmelin Handbook: B: B-Verb.14, 3.8.1.2.1, page 94 - 97
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Continental Oil Co.
Patent: US3136820 , 1964 ;
C. A., 1964 , vol. 61, p. 6919
