反应条件
in tetrahydrofuran N2-atmosphere; 4 equiv. of Ru-compd.; stirring (room temp., 1 h), evapn.(vac.), washing (hexane), extn. (CH2Cl2), ext. evapn. (vac.), column ch romy. (SiO2, hexane (Ru3(CO)12), hexane 6/1 and 4/1), combined 2nd and 3rd band hydrogenation; preparative TLC (SiO2, hexane/CH2Cl2 4/1), 1st band (Ru3(CO)12), 2nd band (Ru4-compd.), 3rd band (1st product, recrystn. from hexane/CH2Cl2 at 4°C), 4th band (2nd product);
参考文献
Organometallics, , vol. 16, p. 689 - 694
