4-丁基-N,N-二甲基苯胺合成路线 （共 9 条）
反应条件
Pd[P(t-Bu)3]2 in toluene T=20°C; Schlenk techniqueInert atmosphere;
参考文献
Giannerini, Massimo; Fananas-Mastral, Martin; Feringa, Ben L.
Nature Chemistry, 2013 , vol. 5, # 8 p. 667 - 672
反应条件
1: (s)-pinanediol butylboronate With sec.-butyllithium in tetrahydrofuran; cyclohexane T=-78 - 20°C; Suzuki-Miyaura reaction; 1.5 h; 2: 4-bromo-N,N-dimethyl-aniline With sodium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in tetrahydrofuran T=70 - 80°C;
参考文献
Zou, Gang; Falck
Tetrahedron Letters, 2001 , vol. 42, # 34 p. 5817 - 5819
反应条件
dimethylsulfide borane complex in tetrahydrofuran T=20°C;
参考文献
Wei, Tiezheng; Lan, Yu; Xu, Jiaxi
Heteroatom Chemistry, 2005 , vol. 16, # 1 p. 2 - 5
反应条件
tripotassium phosphate monohydrate; chloro(2-dicyclohexylphosphino-2',4',6'-triisopropyl-1,1'-biphenyl)[2-(2'-amino-1,1'-biphenyl)]palladium(II) in tetrahydrofuran T=110°C; 16 h; Inert atmosphere;
参考文献
Lee, Brian K.; Biscoe, Mark R.; Buchwald, Stephen L.
Tetrahedron Letters, 2009 , vol. 50, # 26 p. 3672 - 3674
反应条件
N,N,N',N,-tetramethylethylenediamine; ((Me)N2N)Ni-Cl in tetrahydrofuran T=20°C; Kumada-Corriu-Tamao coupling reaction; 2 h; Inert atmosphere;
参考文献
Vechorkin, Oleg; Proust, Valerie; Hu, Xile
Journal of the American Chemical Society, 2009 , vol. 131, # 28 p. 9756 - 9766
反应条件
Ni(acac)2; (Z)-3,3-dimethyl-1,2-bis(diphenylphosphino)-1-butene in CPME 12 h; Inert atmosphereReflux;
参考文献
Kanemura, Shigenari; Kondoh, Azusa; Yorimitsu, Hideki; Oshima, Koichiro
Synthesis, 2008 , # 16 art. no. C02708SS, p. 2659 - 2664
反应条件
sodium cyanoborohydride; acetic acid T=20°C; Inert atmosphere;
参考文献
Chiranjeevi, Barreddi; Koyyada, Ganesh; Prabusreenivasan; Kumar, Vanaja; Sujitha, Pombala; Kumar, C. Ganesh; Sridhar; Shaik, Saida; Chandrasekharam, Malapaka
RSC Advances, 2013 , vol. 3, # 37 p. 16475 - 16485
反应条件
ethanol; nickel Hydrogenation;
参考文献
Rupe; Collin; Schmiderer
Helvetica Chimica Acta, 1931 , vol. 14, p. 1340,1348
参考文献
Davies; Hulbert
Journal of the Society of Chemical Industry, London, 1938 , vol. 57, p. 349
