3-(溴甲基)-5-甲氧基苯甲酸甲酯合成路线 （共 3 条）
反应条件
phosphorus tribromide in dichloromethane T=20°C; 1 h;
参考文献
Genetech, Inc.; Curis, Inc.; Cai, Xiong; Qian, Changgeng; Zhai, Haixiao
Patent: US2014/18368 A1, 2014 ;
Location in patent: Paragraph 0162; 0250 ;
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in tetrachloromethane HeatingIrradiation;
参考文献
Deshpande, Prashant P.; Martin, Olivier R.
Tetrahedron Letters, 1990 , vol. 31, # 44 p. 6313 - 6316
反应条件
1: diisobutylaluminium hydride / tetrahydrofuran / 20 °C 2: phosphorus tribromide / dichloromethane / 1 h / 20 °C View Scheme
