苯甲基-2-乙酰氨基-4,6-O-苯亚甲基-2-脱氧-Alpha-D-吡喃葡萄糖苷合成路线 （共 20 条）
反应条件
toluene-4-sulfonic acid in N,N-dimethyl-formamide T=20°C; 3 h;
参考文献
Journal of Carbohydrate Chemistry, , vol. 32, # 5-6 p. 392 - 409
→
13343-61-8N-[(4aR,6R,7R,8R,8aS)-6-苄氧基-8-羟基-2-苯基-4,4A,6,7,8,8A-六氢吡喃并[5,6-d][1,3]二恶英-7-基]乙酰胺+
反应条件
toluene-4-sulfonic acid in N,N-dimethyl-formamide T=55°C;
参考文献
WO2012/103990 A1, ;
Page/Page column 45 ;
反应条件
trifluorormethanesulfonic acid; orthoformic acid triethyl ester in 1,4-dioxane; N,N-dimethyl-formamide 8 h; Ambient temperature;
参考文献
Carbohydrate Research, , vol. 251, p. 269 - 284
反应条件
diborane in tetrahydrofuran T=0°C; 2.5 h;
参考文献
Chemische Berichte, , vol. 113, # 9 p. 3089 - 3093
反应条件
in pyridine; methanol; chloroform T=0°C; 12 h;
参考文献
, vol. 1986, # 1 p. 37 - 45
反应条件
diborane in tetrahydrofuran T=0°C; 2.5 h;
参考文献
Chemische Berichte, , vol. 113, # 9 p. 3089 - 3093
反应条件
toluene-2-sulfonic acid; orthoformic acid triethyl ester in 1,4-dioxane; N,N-dimethyl-formamide 20 h; Ambient temperature;
参考文献
, vol. 1986, # 1 p. 37 - 45
反应条件
toluene-4-sulfonic acid in benzene 4 h; Heating;
参考文献
Synthesis, , # 1 p. 29 - 32
反应条件
1: 18 percent / NaN3 / dimethylformamide; H2O / 1 h / Heating; further reagents: KOtBu, DBN 2: 35 percent / B2H6 / tetrahydrofuran / 2.5 h / 0 °C View Scheme
参考文献
Chemische Berichte, , vol. 113, # 9 p. 3089 - 3093
反应条件
1: 53 percent / acetyl chloride / 4 h / 75 °C 2: 58 percent / 10 percent H2SO4 / methanol / 0.05 h / 100 °C View Scheme
参考文献
Russian Journal of Bioorganic Chemistry, , vol. 25, # 9 p. 628 - 634
