反应条件
1: 62.2 percent / tosyl azide, triethylamine / acetonitrile / 36 h / Ambient temperature
2: 45.5 percent / CuSO4, Cu(acac)2 / benzene / 24 h / Heating
3: 28.8 percent / 580 - 600 °C / 0.01 Torr
4: 60.5 percent / LiI / dimethylformamide / 2.5 h / Heating
View Scheme
参考文献
Hudlicky, Tomas; Reddy, D. Bhaskar; Govindan, S. V.; Kulp, Thomas; Still, Bobbi; Sheth, Jagdish P.
Journal of Organic Chemistry, 1983 , vol. 48, # 20 p. 3422 - 3428