反应条件
1.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 20 °C / Inert atmosphere 2.1: hydroxylamine hydrochloride; sodium hydrogencarbonate / ethanol / 1 h / 20 °C / Inert atmosphere 3.1: hydrogenchloride; Pearlman's catalyst; hydrogen / methanol; water / 12 h / 30 °C / 760.05 Torr 4.1: triethylamine / N,N-dimethyl-formamide / 1 h / 0 °C / Inert atmosphere 5.1: manganese(IV) oxide / dichloromethane / 20 °C / Inert atmosphere 6.1: 4-(N,N-dimethlyamino)pyridine; triethylamine / dichloromethane / 0.5 h / 20 °C / Inert atmosphere 7.1: boron trifluoride diethyl etherate / dichloromethane / 0.67 h / -78 °C / Inert atmosphere 7.2: -78 °C / Inert atmosphere 8.1: 1,3,5-trimethyl-benzene / 6 h / 160 - 170 °C / Sealed tube; Inert atmosphere 9.1: acetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone / 1,4-dioxane / 0.5 h / 20 °C / Inert atmosphere 9.2: 1 h / 20 °C / Inert atmosphere 10.1: K2OsO4*2H2O; (DHQD)2-PYR; methanesulfonamide; potassium carbonate; potassium hexacyanoferrate(III) / water; tert-butyl alcohol / 48 h / 0 °C / Inert atmosphere 11.1: iodine; calcium carbonate / methanol; water / 15 h / 40 °C / Inert atmosphere 12.1: hydrogen bromide / water / 5 h / 110 °C / Sealed tube; Inert atmosphere View Scheme
参考文献
Yao, Yuan-Shan; Liu, Jia-Li; Xi, Jie; Miu, Bukeyan; Liu, Guai-Sai; Wang, Shaozhong; Meng, Linghua; Yao, Zhu-Jun
Chemistry - A European Journal, 2011 , vol. 17, # 37 p. 10462 - 10469
