反应条件
1: sodium azide / N,N-dimethyl-formamide / 3 h / 0 °C / Darkness; Inert atmosphere
2: palladium 10 on activated carbon; hydrogen / methanol; ethyl acetate / 4 h / 20 °C / Darkness; Inert atmosphere
View Scheme
参考文献
Donohoe, Timothy J.; Jones, Christopher R.; Kornahrens, Anne F.; Barbosa, Luiz C. A.; Walport, Louise J.; Tatton, Matthew R.; O'Hagan, Michael; Rathi, Akshat H.; Baker, David B.
Journal of Organic Chemistry, 2013 , vol. 78, # 24 p. 12338 - 12350