1,1’-氧基双[3-硝基-5-(三氟甲基)苯]合成路线 （共 11 条）
反应条件
potassium fluoride in N-methyl-acetamide; water
参考文献
Occidental Chemical Corporation
Patent: US5122613 A1, 1992 ;
反应条件
KNO2 in N,N-dimethyl-formamide T=130 - 140°C; 20 h;
参考文献
Khalfina; Rogozhnikova; Vlasov
Russian Journal of Organic Chemistry, 1996 , vol. 32, # 9 p. 1325 - 1331
反应条件
KNO2 in N,N-dimethyl-formamide T=130 - 140°C; 20 h;
参考文献
Khalfina; Rogozhnikova; Vlasov
Russian Journal of Organic Chemistry, 1996 , vol. 32, # 9 p. 1325 - 1331
反应条件
3,5-Dinitrobenzotrifluoride; potassium carbonate in N,N-dimethyl-formamide T=85 - 145°C; 17 h;
参考文献
Khalfina; Rogozhnikova; Vlasov
Russian Journal of Organic Chemistry, 1996 , vol. 32, # 9 p. 1325 - 1331
反应条件
KNO2; potassium carbonate in N,N-dimethyl-formamide T=95°C; 3 h;
参考文献
Khalfina; Rogozhnikova; Vlasov
Russian Journal of Organic Chemistry, 1996 , vol. 32, # 9 p. 1325 - 1331
反应条件
potassium carbonate in N,N-dimethyl-formamide T=85 - 145°C; 17 h;
参考文献
Khalfina; Rogozhnikova; Vlasov
Russian Journal of Organic Chemistry, 1996 , vol. 32, # 9 p. 1325 - 1331
反应条件
1: 69 percent / NaI, glacial acetic acid / acetone / 24 h / 63 - 65 °C 2: 77 percent / KF, o-phthaloyl dichloride / tetrahydrothiophene 1,1-dioxide / 24 h / 180 - 200 °C 3: 40 percent / KNO2 / dimethylformamide / 20 h / 130 - 140 °C View Scheme
参考文献
Khalfina; Rogozhnikova; Vlasov
Russian Journal of Organic Chemistry, 1996 , vol. 32, # 9 p. 1325 - 1331
反应条件
KNO2 in N,N-dimethyl-formamide T=130 - 140°C; 20 h;
参考文献
Khalfina; Rogozhnikova; Vlasov
Russian Journal of Organic Chemistry, 1996 , vol. 32, # 9 p. 1325 - 1331
反应条件
potassium carbonate in N,N-dimethyl-formamide T=130 - 140°C; 17 h;
参考文献
Khalfina; Rogozhnikova; Vlasov
Russian Journal of Organic Chemistry, 1996 , vol. 32, # 9 p. 1325 - 1331
反应条件
hydrazine hydrate; palladium in ethanol
参考文献
Occidental Chemical Corporation
Patent: US5122613 A1, 1992 ;
