n-butyllithium; potassium tert-butylate in hexane 96 h; Heating;

n-butyllithium; potassium tert-butylate in hexane 96 h; Heating;

<b>Multi-step reaction with 2 steps<br /> </b>1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 20 &deg;C / |Inert atmosphere<br />1.2: 1 h / 20 &deg;C / |Inert atmosphere<br />2.1: potassium carbonate; palladium diacetate; trimethylbenzylammonium bromide / N,N-dimethyl-formamide / 9 h / 120 &deg;C / |Inert atmosphere<br /> <br /> &nbsp;

<b>Multi-step reaction with 2 steps<br /> </b>1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 20 &deg;C / |Inert atmosphere<br />1.2: 1 h / 20 &deg;C / |Inert atmosphere<br />2.1: potassium carbonate; palladium diacetate; trimethylbenzylammonium bromide / N,N-dimethyl-formamide / 9 h / 120 &deg;C / |Inert atmosphere<br /> <br /> &nbsp;