1,1'-[1,3-亚苯基二(亚甲基)]二-1,4,7,10-四氮杂环十二烷辛盐酸盐合成路线 （共 9 条）
反应条件
1: hydrazine monohydrate View Scheme
参考文献
Brandes, Stephane
Bulletin de la Societe Chimique de France, 1996 , vol. 133, # 1 p. 65 - 73
反应条件
1: 90 percent / H2 / Pd/C View Scheme
参考文献
Kimura, Eiichi; Aoki, Shin; Koike, Tohru; Shiro, Motoo
Journal of the American Chemical Society, 1997 , vol. 119, # 13 p. 3068 - 3076
反应条件
1: 90 percent / acetonitrile / 24 h / 20 °C 2: 85 percent / hydrazine monohydrate / 120 °C View Scheme
参考文献
Costa, Jerome; Balogh, Edina; Turcry, Veronique; Tripier, Raphael; Le Baccon, Michel; Chuburu, Francoise; Handel, Henri; Helm, Lothar; Toth, Eva; Merbach, Andre E.
Chemistry - A European Journal, 2006 , vol. 12, # 26 p. 6841 - 6851
反应条件
1: 95 percent / H2O; methanol / 3 h / 20 °C 2: 90 percent / acetonitrile / 24 h / 20 °C 3: 85 percent / hydrazine monohydrate / 120 °C View Scheme
参考文献
Le Baccon; Chuburu; Toupet; Handel; Soibinet; Dechamps-Olivier; Barbier; Aplincourt
New Journal of Chemistry, 2001 , vol. 25, # 9 p. 1168 - 1174
反应条件
1: 73 percent / K2CO3 / acetonitrile / 72 h 2: aq. NaOH / 4 h / 80 °C View Scheme
参考文献
Boldrini; Giovenzana; Pagliarin; Palmisano; Sisti
Tetrahedron Letters, 2000 , vol. 41, # 33 p. 6527 - 6530
反应条件
in chloroform T=20°C;
参考文献
Fujioka, Haruto; Kishida, Sayuri; Ishizu, Takashi; Shiro, Motoo; Kinoshita, Eiji; Koike, Tohru
Bulletin of the Chemical Society of Japan, 2010 , vol. 83, # 3 p. 267 - 272
反应条件
1: 74 percent / sodium carbonate / acetonitrile / 48 h / Heating 2: 85 percent / 6 M HCl / 1 h / 80 °C View Scheme
参考文献
Brandes, Stephane
Bulletin de la Societe Chimique de France, 1996 , vol. 133, # 1 p. 65 - 73
参考文献
Kimura, Eiichi; Aoki, Shin; Koike, Tohru; Shiro, Motoo
Journal of the American Chemical Society, 1997 , vol. 119, # 13 p. 3068 - 3076
反应条件
Yield given. Multistep reaction;
参考文献
Yaouanc, Jean-Jacques; Bris, Nathalie Le; Gall, Guenaelle Le; Clement, Jean-Claude; Handel, Henri; Abbayes, Herve des
Journal of the Chemical Society, Chemical Communications, 1991 , # 4 p. 206 - 207
