反应条件
1: silica gel / hexane; ethyl acetate 2: sodium iodide, chloro(trimethyl)silane / acetonitrile / Heating 3: 95 percent / NaH / tetrahydrofuran / 1 h / Ambient temperature 4: 50 percent / pyridine / CH2Cl2 / 18 h / Ambient temperature 5: 90 percent / acetic aic, 30percent aq. H2O2 / CH2Cl2 / 1 h / 0 °C View Scheme
参考文献
Chordia, Mahendra D.; Narasimhan, Nurani S.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 2 p. 371 - 376
