lithium aluminium tetrahydride in diethyl ether 5 h; Heating;
参考文献
MacCorquodale, Finlay; Walton, John C.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 347 - 352
Cope,A.C.; Nealy,D.L.
Journal of the American Chemical Society, 1965 , vol. 87, # 14 p. 3122 - 3125
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Baggaley,K.H. et al.
Tetrahedron, 1967 , vol. 23, p. 299 - 304
1: Et3N / CH2Cl2 / 1.) ice-bath, 10 min, 2.) gradually warming to room temperature, 30 min
2: LiBr / acetone / 16 h / Heating
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参考文献
MacCorquodale, Finlay; Walton, John C.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 347 - 352
