7,9-二甲氧羰基-2-乙氧羰基-5-甲氧基-1H-吡咯并-[2,3-f]喹啉合成路线 （共 3 条）
反应条件
1: 69 percent / Ce(NH4)2(NO3)6 / acetonitrile; H2O / 0.5 h / -3 °C 2: 63 percent / LiOH*H2O / tetrahydrofuran; H2O / 20.5 h / Ambient temperature; purification with conc. H2SO4 View Scheme
参考文献
Helvetica Chimica Acta, , vol. 76, # 4 p. 1667 - 1673
反应条件
ammonium cerium (IV) nitrate; water in acetonitrile
T=-5°C; 1.58333 h; Cooling with acetone-dry ice;
参考文献
CLF MEDICAL TECHNOLOGY ACCELERATION PROGRAM, INC.
Patent: WO2006/102642 A1, 2006 ;
Location in patent: Page/Page column 10; 17; 1/6 ;
反应条件
ammonium cerium(IV) nitrate in water; acetonitrile
T=-3°C; 0.5 h;
参考文献
Martin, Pierre; Steiner, Eginhard; Auer, Kurt; Winkler, Tammo
Helvetica Chimica Acta, 1993 , vol. 76, # 4 p. 1667 - 1673
