暂无反应条件数据

1: (COCl)2; DMSO; diisopropylethylamine / CH2Cl2 / 1.33 h / -78 °C 2: 777 mg / CHCl3 / 19 h / 0 °C 3: 63 percent / DIBAL / CHCl3; toluene / 2 h / -78 °C 4: 99 percent / Et3N / tetrahydrofuran / 0.5 h / -78 - 0 °C 5: 66 percent / Et2Zn; Pd(PPh3)4 / tetrahydrofuran; toluene / 1 h / 20 °C View Scheme

Dess-Martin periodane in dichloromethane 5 h;