反应条件
1: (2-ethoxy-2-oxoethyl)(diphenyl)[3-triphenyl(phosphonio)phenyl]phosphonium bromide perchlorate With triethylamine in acetonitrile
T=20°C; Wittig olefination; 0.25 h; Inert atmosphere;
2: benzaldehyde in acetonitrile
T=60°C; Wittig olefination; 16 h; Inert atmosphere; optical yield given as percent de;
参考文献
Lebel, Helene; Davi, Michael; Roy, Marie-Noelle; Zeghida, Walid; Charette, Andre B.
Synthesis, 2011 , # 14 art. no. M27311SS, p. 2275 - 2280