反应条件
1.1: cesium fluoride / dichloromethane; water / 16 h / 20 °C 2.1: tetrahydrofuran / 2 h / 20 °C 3.1: dihydrogen peroxide; sodium hydroxide / water / 0 - 20 °C 4.1: Jone's reagent / acetone / 0 - 20 °C 5.1: chlorosulfonic acid / dichloromethane / 0.75 h / 20 °C 6.1: sodium acetate / ethanol / 15 h / Reflux 6.2: 20 h / 20 °C / 760.05 Torr View Scheme
参考文献
Roesner, Stefan; Casatejada, Javier Mansilla; Elford, Tim G.; Sonawane, Ravindra P.; Aggarwal, Varinder K.
Organic Letters, 2011 , vol. 13, # 21 p. 5740 - 5743
