3-(叔丁基二甲基硅氧基)碘苯合成路线 （共 4 条）
反应条件
1H-imidazole in dichloromethane 18 h;
参考文献
Pelter, Andrew; Hussain, Amjad; Smith, Gareth; Ward, Robert S.
Tetrahedron, 1997 , vol. 53, # 11 p. 3879 - 3916
反应条件
in dichloromethane T=0 - 20°C;
参考文献
ASTRAZENECA AB
Patent: WO2003/106420 A1, 2003 ;
Location in patent: Page 27 ;
WO 03/106420 A1
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diisopropylamine in dichloromethane T=60°C; 18 h;
参考文献
Pelter, Andrew; Hussain, Amjad; Smith, Gareth; Ward, Robert S.
Tetrahedron, 1997 , vol. 53, # 11 p. 3879 - 3916
反应条件
KF-Al2O3 (basic) in acetonitrile 0.166667 h; Ambient temperature;
参考文献
Schmittling, Elisabeth A.; Sawyer, J. Scott
Tetrahedron Letters, 1991 , vol. 32, # 49 p. 7207 - 7210
