5-溴-2-甲氧基间苯二酚合成路线 (共 3 条)
反应条件
hydrogen; palladium on activated charcoal in ethyl acetate
参考文献
Green, Kenneth
Journal of Organic Chemistry, 1991 , vol. 56, # 13 p. 4325 - 4326
反应条件
peracetic acid; n-butyllithium; acetic acid in tetrachloromethane; diethyl ether; water; pentane
参考文献
AMERICAN CYANAMID COMPANY
Patent: EP471941 A2, 1992 ;
反应条件
1: With n-butyllithium in pentane
T=-20 - -10°C; 0.25 h;
2: With boric acid trimethyl ester in pentane
T=-30 - 0°C; 0.5 h;
3: in acetic acid
T=-10 - 0°C; 0.5 h; Further stages.;
参考文献
Maes, Dominick; Vervisch, Stijn; De Kimpe, Norbert
Organic Preparations and Procedures International, 2007 , vol. 39, # 4 p. 395 - 415