2-(叔丁基)-4-氯苯酚合成路线 (共 3 条)
反应条件
sulfuric acid T=20°C; 48 h;
参考文献
PHENEX PHARMACEUTICALS AG; STEENECK, Christoph; KINZEL, Olaf; GEGE, Christian; KLEYMANN, Gerald; HOFFMANN, Thomas
Patent: WO2013/79223 A1, 2013 ;
Location in patent: Page/Page column 77 ;
反应条件
2,2,6,6-tetramethyl-piperidine; sulfuryl dichloride in benzene-d6 T=25°C; 0.75 h; Inert atmosphere; Reagent/catalystTimeSolvent; regioselective reaction;
参考文献
Saper, Noam I.; Snider, Barry B.
Journal of Organic Chemistry, 2014 , vol. 79, # 2 p. 809 - 813
反应条件
sulfuryl dichloride; tetrabutyl-ammonium chloride in benzene-d6 T=25°C; 0.0166667 h; Inert atmosphere; Reagent/catalystTimeConcentration;
参考文献
Saper, Noam I.; Snider, Barry B.
Journal of Organic Chemistry, 2014 , vol. 79, # 2 p. 809 - 813