反应条件
1: 1-iodomethyl acetate With chloro-trimethyl-silane; 1,1-dibromo ethane; zinc in tetrahydrofuran
T=0 - 5°C; 1 h;
2: 9-Bn-6-chloropurine With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
T=20°C; Negishi reaction; 8 h;
参考文献
Silhar, Peter; Pohl, Radek; Votruba, Ivan; Hocek, Michal
Organic Letters, 2004 , vol. 6, # 19 p. 3225 - 3228
