1: 1-amino-naphthalene With hydrogenchloride; sodium nitrite in water T=0 - 5°C; 2: With sodium tetrafluoroborate in water 0.166667 h; 3: monophenyl triethoxy silane With tetrabutyl ammonium fluoride; palladium diacetate in water T=25°C; Hiyama Coupling; 6 h;
1: 1-amino-naphthalene With hydrogenchloride in water T=0 - 5°C; 2: With sodium tetrafluoroborate; sodium nitrite in water T=5°C; 0.166667 h; 3: diphenyldimethoxysilane With methanol; palladium diacetate T=25°C; Hiyama coupling; 6 h;
hydrogenchloride; sodium nitrite Eintragen des Reaktionsgemisches in wss. Natriumpolysulfid und Erhitzen des danach erhaltenen Reaktionsprodukts mit wss. NaOH;
参考文献
Tedjamulia, Marvin L.; Tominaga, Yoshinori; Castle, Raymond N.; Lee, Milton L.
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 1143 - 1148
