Orlov, V. D.; Papiashvili, I. Z.; Grigorov, P. A.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , vol. 19, # 5 p. 544 - 549
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , vol. 19, # 5 p. 671 - 676
1: 100 percent Spectr. / CH2Cl2 / 1 h / 0 °C
2: acetyl bromide / acetonitrile
3: 95 percent / benzene / 7 h / Heating
4: phosgene / benzene / a) 0 deg C, 30 min, b) RT, 30 h
5: H2O / tetrahydrofuran / 0.5 h
View Scheme
参考文献
Givens, Richard S.; Athey, Phillip S.; Matuszewski, Bogdan; Kueper III, L. William; Xue, Jie-You; Fister, Thomas
Journal of the American Chemical Society, 1993 , vol. 115, # 14 p. 6001 - 6012
Van Belzen, Ruud; Klein, Rene A.; Smeets, Wilberth J.J.; Spek, Anthony L.; Benedix, Roland; Elsevier, Cornelis J.
Recueil des Travaux Chimiques des Pays-Bas-Journal of the Royal Netherlands, 1996 , vol. 115, # 5 p. 275 - 285
1: 40 percent / benzene / 2 h / Ambient temperature
2: 62 percent / 12M HCl / H2O / 2 h / 160 °C
View Scheme
参考文献
Van Belzen, Ruud; Klein, Rene A.; Smeets, Wilberth J.J.; Spek, Anthony L.; Benedix, Roland; Elsevier, Cornelis J.
Recueil des Travaux Chimiques des Pays-Bas-Journal of the Royal Netherlands, 1996 , vol. 115, # 5 p. 275 - 285
