in tetrahydrofuran
(under N2); addn. of CsF to a suspn. of S3N3(O)2(SnMe3) in THF, stirring for 1 h at 50°C; filtn., drying of the solid, washing, drying, extn., elem. anal.;
参考文献
Witt, M.; Roesky, H. W.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1984 , vol. 515, p. 51 - 60
byproducts: CF3SH, S, CsF*HF; warming to 25°C in the presence of excess CsF;
参考文献
Burton,C.A.; Shreeve,J.M.
Journal of the American Chemical Society, 1976 , vol. 98, p. 6545 - 6547
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Gmelin Handbook: F: PerFHalOrg.SVol.2, 6.2.1.6.5, page 172 - 209
in diethylene glycol
byproducts: FSO2CF2CF2O{CF(CF3)CF2O}(n)CF(CF3)C(O)F n:3-12;; 25-35°C, 4 h, excess of epoxide, the residue is a polymer mixture; distn.;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.3, 6.2.3.4, page 152 - 186
Full Text Show Details
E.I. Du Pont de Nemours & Co.
Patent: US3301893 , 1967 ;
C.A., 1965 , vol. 63, p. 16216
Full Text Show Details
E.I. Du Pont de Nemours & Co.
Patent: FR1406778 , 1967 ;
C.A., 1965 , vol. 63, p. 16216
Chambers, R. D.; Clark, D. T.; Holmes, T. F.; Musgrave, W. K. R.; Ritchie, I.
J. Chem. Soc. Perkin Trans., 1974 , vol. I, p. 114 - 125
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Gmelin Handbook: F: PerFHalOrg.5, 4, page 115 - 148
