in hydrogen fluoride byproducts: BrF; HF (liquid); careful addn. of BrF3 to a HF-soln. of the Ir-compound;; crystn. at -60°C, recrystn. from HF (liquid), elem. anal.;;
参考文献
Zeitschrift fuer Anorganische und Allgemeine Chemie, , vol. 522, p. 7 - 10
in neat (no solvent) byproducts: NH3; reaction with excess of amide in an autoclave at 400-800°C over several days; washing with liquid NH3 at room temp.; elem. anal.;
参考文献
Journal of the Less-Common Metals, , vol. 146, p. 147 - 160
