Sladky, F.
Angewandte Chemie, 1969 , vol. 81, p. 330 - 330
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Sladky, F.
Angewandte Chemie, 1970 , vol. 82, p. 357 - 357
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Gmelin Handbook: He: Edelgasverb., 1.8.7.3, page 126 - 127
in water addn. of CsF to ZrO(NO3)2*2H2O soln. with stirring, homogenization of mixt. addn. of H3PO4 (5 wtpercent ZrO2; F/Zr molar ratio=3.8); pptn. for 7-45 ds, filtration, washing with H2O and EtOH, drying in air;elem. anal.;
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Godneva; Motov; Kuznetsov; Shchur
Russian Journal of Inorganic Chemistry, 2012 , vol. 57, # 4 p. 492 - 498
hydrogen fluoride in hydrogen fluoride addn. at -196°C, stirring at 20° C for 2 h; cooled to -78°C and filtered, most of HF removed by pumping, theresidue warmed to room temp., the volatiles pumped off (NF3 and HF), the solid residue contained CsSbF6;
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Christe, Karl O.; Wilson, William W.; Wilson, Richard D.
Inorganic Chemistry, 1980 , vol. 19, p. 1494 - 1498
Dresdner, R. D.; Tlumac, F. N.; Young, J. A.
Journal of the American Chemical Society, 1960 , vol. 82, p. 5831 - 5834
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Gmelin Handbook: C: MVol.D3, 7.1.1.2, page 268 - 268
methyl iodide in further solvent(s) byproducts: CsI; (Ar); standard Schlenk technique; toluene (1 equiv.), MeI (2 equiv.) and CsF (1.4 equiv.) added to soln. of tin compd. (1 equiv.) in 1-methyl-2-pyrrolidinone under CO2 at 19°C; GC and NMR monitoring; not isolated;
methyl iodide in N,N-dimethyl-formamide; toluene byproducts: (CH3O)2CO, CsI; (Ar); standard Schlenk technique; toluene (1 equiv.), MeI (2 equiv.) and CsF (1.4 equiv.) added to soln. of tin compd. (1 equiv.) in DMF under CO2 at 19°C; GC and NMR monitoring; not isolated;
carbon dioxide; methyl iodide in N,N-dimethyl-formamide; toluene byproducts: CsI; (Ar); standard Schlenk technique; toluene (1 equiv.), MeI (2 equiv.) and CsF (1.4 equiv.) added to soln. of tin compd. (1 equiv.) in DMF under CO2 at 19°C; GC and NMR monitoring; not isolated;
