N,N′-双(2,6-二异丙基苯基)乙二胺合成路线 (共 7 条)
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=0 - 20°C;
参考文献
Thomson, Jennifer E.; Campbell, Craig D.; Concellon, Carmen; Duguet, Nicolas; Rix, Kathryn; Slawin, Alexandra M. Z.; Smith, Andrew D.
Journal of Organic Chemistry, 2008 , vol. 73, # 7 p. 2784 - 2791
反应条件
sodium tetrahydroborate in tetrahydrofuran Heating;
参考文献
Donohoe, Timothy J.; Harris, Robert M.; Butterworth, Sam; Burrows, Jeremy N.; Cowley, Andrew; Parker, Jeremy S.
Journal of Organic Chemistry, 2006 , vol. 71, # 12 p. 4481 - 4489
反应条件
1: H2O; acetone View Scheme
参考文献
Organic letters, , vol. 1, # 6 p. 953 - 956
反应条件
1: 2: With sodium tetrahydroborate in ethanol
参考文献
Organometallics, , vol. 31, # 24 p. 8505 - 8515
反应条件
in neat (no solvent) inert atmosphere; 90°C, 1 h; evapn. of volatiles (reduced pressure), extn. (hexane), filtration, partial evapn., crystn.;
参考文献
Inorganic Chemistry, , vol. 30 - 11, p. 2487 - 2494
反应条件
4-methyl-morpholine; phosphorus trichoride in tetrahydrofuran T=-78 - 20°C; 20 h;
参考文献
Caputo, Christine A.; Price, Jacquelyn T.; Jennings, Michael C.; McDonald, Robert; Jones, Nathan D.
Dalton Transactions, 2008 , # 26 p. 3461 - 3469
反应条件
triethylamine; phosphorus trichoride in dichloromethane
参考文献
Caputo, Christine A.; Price, Jacquelyn T.; Jennings, Michael C.; McDonald, Robert; Jones, Nathan D.
Dalton Transactions, 2008 , # 26 p. 3461 - 3469