6,6,7,7,8,8,9,9,10,10,11,11,11-十三氟-1-十一烷醇合成路线 （共 6 条）
→
134052-02-16,6,7,7,8,8,9,9,10,10,11,11,11-十三氟-1-十一烷醇
反应条件
hydrogenchloride; zinc in ethanol
参考文献
Sun, Jian-Ying; Li, Jing; Qiu, Xiao-Long; Qing, Feng-Ling
Journal of Fluorine Chemistry, 2005 , vol. 126, # 9-10 p. 1425 - 1431
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134052-02-16,6,7,7,8,8,9,9,10,10,11,11,11-十三氟-1-十一烷醇
反应条件
1.1: Na / diethyl ether / 2 h / Heating 1.2: 90 percent / H2O 2.1: 90 percent / AIBN / 80 °C 3.1: 76 percent / H2; diethylamine / 5 percent Pd/C / ethanol; ethyl acetate / 0.5 h / 9120 Torr View Scheme
参考文献
Tra Anh; Blancou; Commeyras
Journal of Fluorine Chemistry, 1999 , vol. 96, # 2 p. 167 - 174
→
134052-02-16,6,7,7,8,8,9,9,10,10,11,11,11-十三氟-1-十一烷醇
反应条件
1: 90 percent / AIBN / 80 °C 2: 76 percent / H2; diethylamine / 5 percent Pd/C / ethanol; ethyl acetate / 0.5 h / 9120 Torr View Scheme
参考文献
Tra Anh; Blancou; Commeyras
Journal of Fluorine Chemistry, 1999 , vol. 96, # 2 p. 167 - 174
→
134052-02-16,6,7,7,8,8,9,9,10,10,11,11,11-十三氟-1-十一烷醇
反应条件
1: 75 percent / AIBN / 95 °C 2: 85 percent / Zn; HCl / ethanol View Scheme
参考文献
Greiner, J.; Milius, A.; Riess, J. G.
Journal of Fluorine Chemistry, 1992 , vol. 56, # 3 p. 285 - 293
→
134052-02-16,6,7,7,8,8,9,9,10,10,11,11,11-十三氟-1-十一烷醇
反应条件
1: 75 percent / AIBN / 95 °C 2: 85 percent / Zn; HCl / ethanol View Scheme
参考文献
Greiner, J.; Milius, A.; Riess, J. G.
Journal of Fluorine Chemistry, 1992 , vol. 56, # 3 p. 285 - 293
→
134052-02-16,6,7,7,8,8,9,9,10,10,11,11,11-十三氟-1-十一烷醇
反应条件
hydrogenchloride; zinc
参考文献
Leveque, Laurence; Le Blanc, Maurice; Pastor, Raphael
Tetrahedron Letters, 1997 , vol. 38, # 34 p. 6001 - 6002
