2-氯-1-(4-硝基苯基)乙醇合成路线 (共 4 条)
反应条件
1: chloromethyl iodide With isopropylmagnesium chloride lithium chloride complex in tetrahydrofuran T=-78°C; 0.166667 h; Inert atmosphere; 2: 4-nitrobenzaldehdye in tetrahydrofuran T=-78 - 20°C; 0.5 h; Inert atmosphere;
参考文献
Nishimura, Rodolfo H.V.; Toledo, Fabiano T.; Lopes, Joao L.C.; Clososki, Giuliano C.
Tetrahedron Letters, 2013 , vol. 54, # 4 p. 287 - 290
反应条件
lithium chloride; copper dichloride in tetrahydrofuran T=20°C; Inert atmosphere;
参考文献
Haak, Robert M.; Berthiol, Florian; Jerphagnon, Thomas; Gayet, Arnaud J. A.; Tarabiono, Chiara; Postema, Christiaan P.; Ritleng, Vincent; Pfeffer, Michel; Janssen, Dick B.; Minnaard, Adriaan J.; Feringa, Ben L.; De Vries, Johannes G.
Journal of the American Chemical Society, 2008 , vol. 130, # 41 p. 13508 - 13509
反应条件
sodium tetrahydroborate in methanol T=20°C;
参考文献
Bisogno, Fabricio R.; Lavandera, Ivan; Kroutil, Wolfgang; Gotor, Vicente
Journal of Organic Chemistry, 2009 , vol. 74, # 4 p. 1730 - 1732
参考文献
Terada
Nippon Kagaku Zasshi, 1955 , vol. 76, p. 1282,1283
Chem.Abstr., 1957 , p. 17807