(1S,2S)-(+)-2-甲氧基环己醇合成路线 (共 26 条)
反应条件
Amberlite IRA-900; hydrogen; Pt/Al2O3; (-)-4-[(R)-((2S)-5-ethyl-1-azabicyclo[2.2.2]oct-2-yl)-methoxy-methyl]-quinoline in acetic acid T=25°C; P=45004.5 Torr; 0.266667 h; Product distributionKinetics; Further Variations:CatalystsSolventsReagents;
参考文献
Advanced Synthesis and Catalysis, , vol. 344, # 5 p. 511 - 515
反应条件
methanol; boron trifluoride
参考文献
Zhurnal Obshchei Khimii, , vol. 10, p. 981,988
Chem. Zentralbl., , vol. 112, # I p. 764
反应条件
hydrogenchloride; methanol
参考文献
Journal of the American Chemical Society, , vol. 65, p. 2199
Justus Liebigs Annalen der Chemie, , vol. 510, p. 129,134, 136
Justus Liebigs Annalen der Chemie, , vol. 516, p. 231,239
反应条件
1: glacial acetic acid / 110 °C 2: methanol; concentrated aqueous HCl View Scheme
参考文献
Journal of the American Chemical Society, , vol. 65, p. 2199
Justus Liebigs Annalen der Chemie, , vol. 510, p. 129,134, 136
Justus Liebigs Annalen der Chemie, , vol. 516, p. 231,239
参考文献
Kas'yan, L. I.; Stepanova, N. V.; Belyakova, T. A.; Kunanets, V. K.; Lutsenko, A. I.; Zefirov, N. S.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, # 11 p. 2090 - 2095
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 11 p. 2295 - 2301
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Journal of the American Chemical Society, , vol. 80, p. 2237,2241
反应条件
in methanol Ring cleavage; 6 h; Heating;
参考文献
Kassai, Csaba; Juvancz, Zoltan; Balint, Jozsef; Fogassy, Elemer; Kozma, David
Tetrahedron, 2000 , vol. 56, # 42 p. 8355 - 8359
反应条件
in dichloromethane T=20°C; 0.0833333 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 822 - 827
反应条件
methanol; sodium methylate T=50°C; anfangs unter Kuehlung;
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 205, p. 327
Bulletin de la Societe Chimique de France, , p. 459,460
反应条件
methanol; dihydrogen peroxide; tungsten(VI) trioxide hydrate
参考文献
Journal of Organic Chemistry, , vol. 22, p. 1680