(1S,2S)-(+)-2-甲氧基环己醇合成路线 (共 26 条)
反应条件
NiCRA-MgBr2 (2,5-dimethylhexanol, NaH, Ni(OAc)2, MgBr2) in tetrahydrofuran T=63°C; 66 h; other complex reducing agents; thermodynamic equilibration; other methoxycyclohexanols; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 55, # 23 p. 5916 - 5919
反应条件
iodosylbenzene; bleomycin A2; iron(III) cation in methanol 1 h; Ambient temperature; Product distribution;
参考文献
Journal of the American Chemical Society, , vol. 107, # 2 p. 493 - 500
反应条件
(i) TlOEt, benzene, (ii) /BRN= 969135/, MeCN; Multistep reaction;
参考文献
Angewandte Chemie, , vol. 87, # 22 p. 812 - 813
反应条件
Erhitzen des Reaktionsprodukts auf 130grad;
参考文献
Archiv der Pharmazie (Weinheim, Germany), , vol. 289, p. 673,676
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 233, p. 484
Annales de Chimie (Cachan, France), , vol. <12> 8, p. 5,10
反应条件
chromium(VI) oxide; sulfuric acid in dichloromethane; water
T=0°C; 1 h;
参考文献
Rossi, Tino; Marchioro, Carla; Paio, Alfrede; Thomas, Russell J.; Zarantonello, Paola
Journal of Organic Chemistry, 1997 , vol. 62, # 6 p. 1653 - 1661