2-[3-乙酰氧基-2-(甲氧基甲基)-5-(2-甲氧基-2-氧代乙氧基)四氢吡喃-4-基]氧基乙酸甲酯合成路线 （共 4 条）
反应条件
1: 75 percent / NaH / dimethylformamide / 2 h / 110 °C 2: 62 percent / LiAlH4, AlCl3 / diethyl ether; CH2Cl2 / 0.17 h / Heating 3: 90 percent / methylation 4: 65 percent / 50percent HOAc / 18 h / 70 °C View Scheme
参考文献
Zeller, Samuel G.; Griesgraber, George W.; Gray, Gary R.
Carbohydrate Research, 1991 , vol. 211, # 1 p. 47 - 57
反应条件
1: 62 percent / LiAlH4, AlCl3 / diethyl ether; CH2Cl2 / 0.17 h / Heating 2: 90 percent / methylation 3: 65 percent / 50percent HOAc / 18 h / 70 °C View Scheme
参考文献
Zeller, Samuel G.; Griesgraber, George W.; Gray, Gary R.
Carbohydrate Research, 1991 , vol. 211, # 1 p. 47 - 57
反应条件
1: 90 percent / methylation 2: 65 percent / 50percent HOAc / 18 h / 70 °C View Scheme
参考文献
Zeller, Samuel G.; Griesgraber, George W.; Gray, Gary R.
Carbohydrate Research, 1991 , vol. 211, # 1 p. 47 - 57
参考文献
Zeller, Samuel G.; Griesgraber, George W.; Gray, Gary R.
Carbohydrate Research, 1991 , vol. 211, # 1 p. 47 - 57
