反应条件
1: (1S,6R)-diethyl 5-oxo-3-oxabicyclo[4.1.0]heptane-7,7-dicarboxylate With sodium tetrahydroborate in tetrahydrofuran T=20 - 60°C; 6 h; Inert atmosphere; 2: methanol in tetrahydrofuran T=60°C; 1.16667 h; Inert atmosphere; 3: With acetic acid in tetrahydrofuran; methanol T=0°C; Inert atmosphere;
参考文献
Shimokawa, Jun; Harada, Takaaki; Yokoshima, Satoshi; Fukuyama, Tohru
Journal of the American Chemical Society, 2011 , vol. 133, # 44 p. 17634 - 17637