O-(2-甲基烯丙基氧基)硝基苯合成路线 （共 6 条）
反应条件
sodium hydride in N,N-dimethyl-formamide T=20°C; 6.5 h;
参考文献
Bunce, Richard A.; Herron, Derrick M.; Hale, Lu Y.
Journal of Heterocyclic Chemistry, 2003 , vol. 40, # 6 p. 1031 - 1039
反应条件
4 A molecular sieve; potassium carbonate in N,N-dimethyl-formamide T=80°C; 34 h;
参考文献
Raeppel, Stephane; Raeppel, Franck; Suffert, Jean
Synlett, 1998 , # 7 p. 794 - 796
反应条件
sodium hydroxide in water T=84°C; 4 h;
参考文献
Gale, Jonathan B.; Klucik, Jozef; Subramanian, Shankar; Berlin, K. Darrell
Organic Preparations and Procedures International, 2001 , vol. 33, # 5 p. 487 - 499
反应条件
1.1: O3 / methanol / -78 °C 1.2: Me2S; p-CH3C6H4SO3H / methanol / 4 h / -78 - 20 °C 1.3: 93 percent / amberlyst-15 / acetone / 12 h / 20 °C 2.1: 92 percent / H2 / Pd/C / methanol / 6 h / 25 °C / 3040 Torr View Scheme
参考文献
Bunce, Richard A.; Herron, Derrick M.; Hale, Lu Y.
Journal of Heterocyclic Chemistry, 2003 , vol. 40, # 6 p. 1031 - 1039
反应条件
1: With ozone in methanol T=-78°C; 2: With dimethylsulfide; toluene-4-sulfonic acid in methanol T=-78 - 20°C; 4 h; 3: With amberlyst-15 in acetone T=20°C; 12 h;
参考文献
Journal of Heterocyclic Chemistry, , vol. 40, # 6 p. 1031 - 1039
反应条件
hydrogenchloride; tin(ll) chloride in ethanol
T=20°C; 18 h;
参考文献
Gale, Jonathan B.; Klucik, Jozef; Subramanian, Shankar; Berlin, K. Darrell
Organic Preparations and Procedures International, 2001 , vol. 33, # 5 p. 487 - 499
