sulfuric acid; dichromate(VI)(2-)

暂无反应条件数据

sulfuric acid; dichromate(VI)(2-) bei der Verseifung des entstehenden 3-Methoxy-benzophenon mit Bromwasserstoffsaeure;

palladium 10 on activated carbon; hydrogen in ethanol; ethyl acetate T=20°C; 5 h;

1.1: Jone's reagent 2.1: n-butyllithium; N,N,N',N,-tetramethylethylenediamine / tetrahydrofuran; hexane / 0.05 h / -98 °C / Inert atmosphere 2.2: 2 h / -98 - -60 °C / Inert atmosphere 2.3: Inert atmosphere 3.1: Cl2Ni(1,2-bis(diphenylphosphino)ethane); 1,1-dimethylethylmagnesium chloride / tetrahydrofuran; dichloromethane / 20 °C / Inert atmosphere 3.2: 20 °C / Inert atmosphere 4.1: diisopropyl-carbodiimide / dichloromethane / 24 h / 25 °C / Inert atmosphere View Scheme