反应条件
CH3COONa/CH3COOH-buffer in 1,4-dioxane refluxing of mixt. (8h), cooling to room temp., addn. of CH3COONa/CH3COOH, further reflux (2h); cooling, pouring onto H2O, extn. (CHCl3), washing of organic layer (aq. NaHCO3), drying (MgSO4), evapn. (vacuo), distn.;
参考文献
Bryce, Martin R.; Fakley, Martin E.
Synthetic Communications, 1988 , vol. 18, # 2 p. 181 - 184
