1-(3-羟基苄基)-3-[4-(吡啶-4-基)噻唑-2-基]脲合成路线 （共 4 条）
反应条件
triethylamine in dichloromethane
T=0 - 20°C; Inert atmosphereAutoclave;
参考文献
Pireddu, Roberta; Forinash, Kara D.; Sun, Nan N.; Martin, Mathew P.; Sung, Shen-Shu; Alexander, Brian; Zhu, Jin-Yi; Guida, Wayne C.; Schoenbrunn, Ernst; Sebti, Said M.; Lawrence, Nicholas J.
MedChemComm, 2012 , vol. 3, # 6 p. 699 - 709
反应条件
1: ethanol / 0.5 h / 100 °C / |Microwave irradiation
2: pyridine / dichloromethane / 0 - 20 °C / |Inert atmosphere
3: tetrahydrofuran; acetonitrile / 0.33 h / 100 °C / 11377.6 Torr / |Microwave irradiation; |Autoclave
4: triethylamine / dichloromethane / 0 - 20 °C / |Inert atmosphere; |Autoclave
View Scheme
参考文献
Pireddu, Roberta; Forinash, Kara D.; Sun, Nan N.; Martin, Mathew P.; Sung, Shen-Shu; Alexander, Brian; Zhu, Jin-Yi; Guida, Wayne C.; Schoenbrunn, Ernst; Sebti, Said M.; Lawrence, Nicholas J.
MedChemComm, 2012 , vol. 3, # 6 p. 699 - 709
反应条件
1: tetrahydrofuran; acetonitrile / 0.33 h / 100 °C / 11377.6 Torr / |Microwave irradiation; |Autoclave
2: triethylamine / dichloromethane / 0 - 20 °C / |Inert atmosphere; |Autoclave
View Scheme
参考文献
Pireddu, Roberta; Forinash, Kara D.; Sun, Nan N.; Martin, Mathew P.; Sung, Shen-Shu; Alexander, Brian; Zhu, Jin-Yi; Guida, Wayne C.; Schoenbrunn, Ernst; Sebti, Said M.; Lawrence, Nicholas J.
MedChemComm, 2012 , vol. 3, # 6 p. 699 - 709
反应条件
1: pyridine / dichloromethane / 0 - 20 °C / |Inert atmosphere
2: tetrahydrofuran; acetonitrile / 0.33 h / 100 °C / 11377.6 Torr / |Microwave irradiation; |Autoclave
3: triethylamine / dichloromethane / 0 - 20 °C / |Inert atmosphere; |Autoclave
View Scheme
参考文献
Pireddu, Roberta; Forinash, Kara D.; Sun, Nan N.; Martin, Mathew P.; Sung, Shen-Shu; Alexander, Brian; Zhu, Jin-Yi; Guida, Wayne C.; Schoenbrunn, Ernst; Sebti, Said M.; Lawrence, Nicholas J.
MedChemComm, 2012 , vol. 3, # 6 p. 699 - 709
