2-[(二甲基-lambda4-硫代)氨基]-5-硝基吡啶合成路线 （共 3 条）
反应条件
N-chloro-succinimide in dichloromethane T=-20°C; 3 h;
参考文献
Rakitin, O. A.; Vlasova, O. G.; Khmel'nitskii, L. I.; Falyakhov, I. F.; Sobachkina, T. N.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1990 , vol. 26, # 11 p. 1281 - 1283
Khimiya Geterotsiklicheskikh Soedinenii, 1990 , # 11 p. 1536 - 1538
反应条件
trifluoroacetic anhydride in dichloromethane T=-60°C; 3 h; multistep; other reagents : 1.) N-chlorosuccinimide, dimethylsulfide, 2.) P2O5, DMSO, 3.) trifluoromethanesulfonic acid anhydride, DMSO; MechanismProduct distribution;
参考文献
Rakitin, O. A.; Vlasova, O. G.; Khmel'nitskii, L. I.; Falyakhov, I. F.; Sobachkina, T. N.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1990 , vol. 26, # 11 p. 1281 - 1283
Khimiya Geterotsiklicheskikh Soedinenii, 1990 , # 11 p. 1536 - 1538
反应条件
dihydrogen peroxide; trifluoroacetic acid in dichloromethane T=0°C;
参考文献
Rakitin, O. A.; Vlasova, O. G.; Khmel'nitskii, L. I.; Falyakhov, I. F.; Sobachkina, T. N.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1990 , vol. 26, # 11 p. 1281 - 1283
Khimiya Geterotsiklicheskikh Soedinenii, 1990 , # 11 p. 1536 - 1538
