反应条件
1: 2.) NaBH4 / 1.) 2-propanol, reflux, 6 h, 2.) MeOH, RT, 3 h
2: 96 percent / benzene / 1.5 h
3: 93 percent / NH3 gas / Ambient temperature
4: 1.) HCl gas, 2.) Et3N / 1.) toluene, RT, overnight, 2.) 2-propanol, reflux, 3 h
View Scheme
参考文献
Kanno; Yamaguchi; Okamiya; Sunakawa; Takeshita; Naruchi
Chemical and Pharmaceutical Bulletin, 1992 , vol. 40, # 8 p. 2049 - 2054