反应条件
1: 55 percent / NaCNBH3 / methanol / 0.5 h / Ambient temperature; pH = 6
2: CH2Cl2 / 1.) 0 deg C., 15 min, 2.) r. t., 10 min.
3: Bu4NBr / 1,2-dichloro-benzene / 0.25 h / Heating
4: LiAlH4 / diethyl ether / 1 h
5: 65 percent / 6 M HCl / 2 h / Heating
View Scheme
参考文献
Compernolle, Frans; Saleh, M.-Ashty; Toppet, Suzanne; Hoornaert, Georges
Journal of Organic Chemistry, 1991 , vol. 56, # 17 p. 5192 - 5196
