in neat (no solvent) addn. of fluorosulfuric acid to pertechnate salt; sublimation at 100°C in vac. with trapping at -78°C, isolation of crystals, X-ray anal.;
参考文献
Supel, Joanna; Hagenbach, Adelheid; Abram; Seppelt, Konrad
Zeitschrift fur Anorganische und Allgemeine Chemie, 2008 , vol. 634, # 4 p. 646 - 648