1H-苯并咪唑-2-硫醇合成路线 （共 177 条）
反应条件
1: 21 percent / KOH / propan-1-ol; H2O / 18 h / Heating
2: H2 / Raney-Ni / ethanol / 6 h / 2574.3 Torr
View Scheme
参考文献
Agrawal, V. K.; Rao, K. V. B.; Sharma, Satyavan
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. <B> 22, # 8 p. 781 - 784
反应条件
1: 21 percent / KOH / propan-1-ol; H2O / 18 h / Heating
2: H2 / Raney-Ni / ethanol / 6 h / 2574.3 Torr
3: 71 percent / 4 h / Heating
View Scheme
参考文献
Agrawal, V. K.; Rao, K. V. B.; Sharma, Satyavan
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. <B> 22, # 8 p. 781 - 784
反应条件
1: 21 percent / KOH / propan-1-ol; H2O / 18 h / Heating
2: H2 / Raney-Ni / ethanol / 6 h / 2574.3 Torr
3: 65 percent / Heating
View Scheme
参考文献
Agrawal, V. K.; Rao, K. V. B.; Sharma, Satyavan
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. <B> 22, # 8 p. 781 - 784
反应条件
1: NaOH, 30percent H2O2 / H2O
2: 86.3 percent / NaOH / aq. ethanol / 1 h
View Scheme
参考文献
Popov, I. I.; Boroshko, S. L.; Tertov, B. A.; Makarov, S. P.; Simonov, A. M.; Simkin, B. Ya.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 12 p. 1348 - 1352
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , # 12 p. 1673 - 1677
反应条件
1: 41.4 percent / NaOH / ethanol / 15 h / Heating
2: 39 mg / NaOH / ethanol / 13.5 h / 140 °C
View Scheme
参考文献
Sasaki, Tadashi; Shimizu, Ikuo
Heterocycles, 1984 , vol. 22, # 5 p. 1225 - 1230
反应条件
potassium carbonate in N,N-dimethyl-formamide
T=20°C;
参考文献
Ray, Purna C.; Mittapelli, Vasantha; Rohatgi, Amit; Tyagi, Om Dutt
Synthetic Communications, 2007 , vol. 37, # 17 p. 2861 - 2868
反应条件
in methanol
Heating;
参考文献
Farrington,K.J.
Australian Journal of Chemistry, 1964 , vol. 17, p. 230 - 232
反应条件
1: 88 percent / triethylamine / benzene / 4 h
2: 97 percent / aq. 2N NaOH / Heating
View Scheme
参考文献
Belgodere, Elena; Bossio, Ricardo; Cencioni, Roberto; Marcaccini, Stefano; Pepino, Roberto
Journal of Heterocyclic Chemistry, 1984 , vol. 21, p. 1241
反应条件
1: 1.) potassium hydroxide / 1.) water, 3 h, reflux; 2.) n-propanol, 72 h, reflux
2: 75.8 percent / hydrogen / Raney-nickel / ethanol; tetrahydrofuran / 5 h / 1838.8 Torr
View Scheme
参考文献
Rao; Charles; Sharma; et al.
European Journal of Medicinal Chemistry, 1981 , vol. 16, # 1 p. 35 - 38
反应条件
di-tert-butylnitroxide radical; sodium hydride
1.) DMF, 2.) DMF, 70 deg C, 10h, irradiation; Yield given. Multistep reaction;
参考文献
Chen, Qing-Yun; Chen, Mei-Jin
Journal of Fluorine Chemistry, 1991 , vol. 51, # 1 p. 21 - 32
