1H-苯并咪唑-2-硫醇合成路线 （共 177 条）
反应条件
1: alkaline medium
2: N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline (EEDQ) / dimethylformamide / 24 h / Ambient temperature
View Scheme
参考文献
El Sherief; Mahmoud; Abdel Rahman; El Naggar
Journal of the Indian Chemical Society, 1983 , vol. 60, # 1 p. 58 - 60
反应条件
1: 65 percent / NaOH / H2O / Heating
2: 70 percent / Ac2O, Py
3: 45 percent / NaOAc / ethanol / 8 h / Heating
View Scheme
参考文献
Soni, Namita; Barthwal, J. P.; Gupta, T. K.; Bhalla, T. N.; Parmar, S. S.; Bhargava, K. P.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. <B> 22, # 8 p. 785 - 788
反应条件
sodium acetate in acetic acid
Heating;
参考文献
Turkevichand,N.M.; Lymar,O.F.
J. Gen. Chem. USSR (Engl. Transl.), 1961 , vol. 31, # 5 p. 1635 - 1640,1523 - 1527
反应条件
1: 65 percent / NaOH / H2O / Heating
2: 70 percent / Ac2O, Py
3: 60 percent / NaOAc / ethanol / 8 h / Heating
View Scheme
参考文献
Soni, Namita; Barthwal, J. P.; Gupta, T. K.; Bhalla, T. N.; Parmar, S. S.; Bhargava, K. P.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. <B> 22, # 8 p. 785 - 788
反应条件
reconstructed hydrotalcite in ethanol
T=70°C; 3 h; Microwave irradiationCooling; Reagent/catalyst;
参考文献
Cruz-Gonzalez, Deysi Y.; Gonzalez-Olvera, Rodrigo; Angeles-Beltran, Deyanira; Negron-Silva, Guillermo E.; Santillan, Rosa
Synthesis (Germany), 2013 , vol. 45, # 23 p. 3281 - 3287
反应条件
N-ethyl-N,N-diisopropylamine in acetone
T=20°C; 0.05 h; Sonication;
参考文献
Deligeorgiev, Todor; Kaloyanova, Stefka; Lesev, Nedyalko; Vaquero, Juan J.
Ultrasonics Sonochemistry, 2010 , vol. 17, # 5 p. 783 - 788
反应条件
sodium hydroxide; Amberlite IRA-400 chloride form in water; acetone
参考文献
Dalal; Pawar; Mahulikar
Organic Preparations and Procedures International, 2005 , vol. 37, # 6 p. 539 - 546
反应条件
1: KOH / ethanol / 0.17 h / 80 °C
2: 52 percent / ethanol / 4 h
View Scheme
参考文献
Badr, M. Z. A.; Mahmoud, A. M.; Mahgoub, S. A.; Hozien, Z. A.
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, p. 1339 - 1344
反应条件
triethylamine in dichloromethane
Ambient temperature;
参考文献
Kees, Kenneth L.; Caggiano, Thomas J.; Steiner, Kurt E.; Fitzgerald, John J.; Kates, Michael J.; et al.
Journal of Medicinal Chemistry, 1995 , vol. 38, # 4 p. 617 - 628
反应条件
sodium acetate in water
参考文献
Eastman Kodak Company
Patent: US5210209 A1, 1993 ;
