1H-苯并咪唑-2-硫醇合成路线 （共 177 条）
反应条件
reconstructed hydrotalcite in ethanol
T=70°C; 0.333333 h; Microwave irradiationCooling;
参考文献
Cruz-Gonzalez, Deysi Y.; Gonzalez-Olvera, Rodrigo; Angeles-Beltran, Deyanira; Negron-Silva, Guillermo E.; Santillan, Rosa
Synthesis (Germany), 2013 , vol. 45, # 23 p. 3281 - 3287
反应条件
potassium hydroxide in ethanol; sulfuric acid; ethyl acetate
参考文献
Yamanouchi Pharmaceutical Co., Ltd.
Patent: US6642264 B1, 2003 ;
反应条件
1: acetyl chloride; 2-mercaptobenzoimidazole With potassium hydroxide in ethanol
T=20°C; 1 h; Heating / reflux;
2: sulfuric acid T=20°C; 6 h;
参考文献
YAMANOUCHI PHARMACEUTICAL CO. LTD.
Patent: EP1167369 A1, 2002 ;
Location in patent: Page 20 ;
EP 1167369 A1
反应条件
18-crown-6 ether; potassium carbonate; potassium iodide in toluene
12 h; Reflux;
参考文献
Beresneva; Belyakov; Abele; Lukevics
Chemistry of Heterocyclic Compounds, 2011 , vol. 46, # 11 p. 1400 - 1404
参考文献
Chadha,V.K. et al.
Indian Journal of Chemistry, 1969 , vol. 7, p. 769 - 771
反应条件
2: polyphosphoric acid
View Scheme
参考文献
Ogura,H. et al.
Journal of Heterocyclic Chemistry, 1969 , vol. 6, p. 797 - 802
反应条件
in ethanol
4 h; Heating;
参考文献
Krasovskii,A.N.; Kochergin,P.M.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1969 , vol. 5, p. 243 - 245
Khimiya Geterotsiklicheskikh Soedinenii, 1969 , vol. 5, # 2 p. 321 - 324
