反应条件
n-butyllithium in diethyl ether; hexane under inert atmosphere, piperidine in hexane reacted with n-BuLi in hexane, dropwise addn. of GaBr3 in diethyl ether at room temp., refluxed for 30 min, stirred at room temp. for 12 h; evapn. of solvent, taken up in pentane, filtered, evapd. in vac.; elem. anal.;
参考文献
Linti, Gerald; Frey, Ronald; Polborn, Kurt
Chemische Berichte, 1994 , vol. 127, # 8 p. 1387 - 1394
