反应条件
in pentane
byproducts: LiBr; added dioxane at 0°C, added in the dark at 0°C LiCH2CMe3 over 50 min, stirred for 2.5 h at room temperature; filtered, volume reduced, cooled to -30°C, elem. anal.;
参考文献
Uhl, Werner; Klinkhammer, Karl-Wilhelm; Layh, Marcus; Massa, Werner
Chemische Berichte, 1991 , vol. 124, # 2 p. 279 - 284
