in further solvent(s)
byproducts: glyme, Cd(CH3)2; Cd compd. added to GeI4 in 1,2-dibromoethane, standing for 1 h, periodically vented to vac.; after volatile germanes recovered, concd., sepd.;
参考文献
Krause, L. J.; Morrison, J. A.
Journal of the American Chemical Society, 1981 , vol. 103, # 11 p. 2995 - 3001
in neat (no solvent)
byproducts: CF3I; carried out under inert atm.; freshly sublimed GeI4 and Te-compd. allowed to interact at 170°C for 120h, or for 150h at 120, 140 and 150°C; not isolated, monitored by NMR;
参考文献
Ganja, E. A.; Morrison, J. A.
Inorganic Chemistry, 1990 , vol. 29, p. 33 - 38
