potassium cyanide
heating PtCl4 with Se excess at 500 °C in CO2 flow; cooling and repeated heating in vac. tube; boiling with KCN; filtering; washing with water, dild.HCl, alcohol and ether; drying at 130 °C in CO2 flow;
in anhydrous butyl ether
Addn. of organolithium soln. to metal salt.; GC after 2-5h.;
参考文献
Kostitsyna, N. N.; Oreshkin, I. A.; Dolgoplosk, B. A.
Doklady Physical Chemistry (Translation of the physical chemistry section of Doklady Akademii Nauk), 1986 , vol. 286 - 288, p. 10 - 12
Doklady Akademii Nauk SSSR, 1986 , vol. 286, p. 132 - 134
zinc oxide
Irradiation (UV/VIS); ZnO, finely powdered, used as a photosensitizer (sun light);;
参考文献
Gmelin Handbook: Zn: SVol., 241, page 815 - 817
Full Text Show Details
Bhattacharya, A. K.; Dhar, N. R.
Q. J. Indian Chem. Soc., 1927 , vol. 4, p. 299 - 306
in water
reduction with Mg in neutral or acidic soln.;
参考文献
Seubert, K.; Schmidt, A.
Liebigs Annalen der Chemie, 1892 , vol. 267, p. 242
Full Text Show Details
Villiers, A.; Borg, F.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1893 , vol. 116, p. 1525
