tetramethylammonium hydroxide in water
High Pressure; hydrothermal conditions; aq. solns. of FeCl3*6H2O and PtCl4 (5 mol.-percent) mixed; soln. of Me4NOH added; mixt. shaken for ca. 10 min; heated at 160°C in Parr bomb for 16 h; cooled to room temp.; ppt. washed with H2O; centrifugation; dried; X-ray powder diffraction, Moessbauer and IR spectra;
参考文献
Krehula, Stjepko; Music, Svetozar
Journal of Molecular Structure, 2011 , vol. 993, # 1-3 p. 382 - 389
in neat (no solvent)
byproducts: HCl; PtCl4 reduced by H2 in sealed glass ampoule at 293 K, 1 atm.;
参考文献
Chusova, Tamara P.; Semenova, Zinaida I.
Thermochimica Acta, 2008 , vol. 469, # 1-2 p. 59 - 64
→
反应条件
in water
byproducts: HCl; 1percent aq. soln. of PtCl4;;
参考文献
Kahlenberg, L.; Steinle, J. V.
Trans. Am. electrochem. Soc., 1923 , vol. 44, p. 493 - 516
Full Text Show Details
Gmelin Handbook: As: MVol., 51, page 181 - 184
