in dichloromethane Sonication; to a Ag-compound P4 in CS2 was added at room temp., volatiles were removed, dissolved in CH2Cl2, I2 was sublimed into the mixt., the soln. was stirred overnight at -30°C; volatiles were removed in vac., extd. with CS2 at room temp.;
参考文献
Journal of the Chemical Society, Dalton Transactions, , # 4 p. 500 - 512
in neat (no solvent) Irradiation (UV/VIS); reversible react. of PI3 with PCl2I in the system PCl3#PI3 by irradiation with light (4385 Å, Hg lamp); equilibrium react.;;
参考文献
Schilling, G.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1957 , vol. 245, p. 2499 - 2502
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Gmelin Handbook: P: MVol.C, 231, page 529 - 530
